Development of electrodeposited nanostructural poly (o-aminophenol) coating as a solid phase microextraction fiber for determination of bisphenol A

ZnO polythiophene SBA-15 nanoparticles as a solid-phase microextraction fiber for fast determination essential oils of Matricaria chamomilla

The objective of this study is determination the volatile compounds of Matricaria chamomilla of an inorganic–organic hybrid material based on ZnO nanoparticles anchored to a composite made from polythiophene and hexagonally ordered silica (ZnO/PT/SBA-15) as a solid-phase fiber microextraction (SPME). Microextraction techniques with nanoparticles ZnO/PT/SBA-15 resulted in a more efficient analyt...

HCl- Etched Steel Fiber for Determination of Phthalates in Water Samples by Solid-Phase Microextraction

In the present work, a stainless steel wire was etched by hydrochloric acid during a chemical etching process. The obtained black layer on the surface of the fiber was used as sorbent for extraction of trace amount of phthalates in the aqueous samples by solid phase microextraction. New fiber efficiency was investigated using a home-made solid-phase microextraction (SPME) device and gas chr...

Carbon nanocones/disks as new coating for solid-phase microextraction.

In this article, the potential of carbon nanocones/disks as coating for solid-phase microextraction has been evaluated for the first time. The nanostructures were immobilized on a stainless steel needle by means of an organic binder. The fiber coating obtained was ca. 50 microm of thickness and 35 mm in length. The evaluation of the sorbent capacity was carried out through the determination of ...

Simultaneous determination of blockers and agonists by on-fiber derivatization in self-made solid-phase microextraction coating fiber.

An environmentally friendly and sensitive method for determination of blockers and agonists was described in this paper. The method is based on a homemade sol-gel solid-phase microextraction (SPME) coating with simultaneous on-fiber derivatization and subsequent gas chromatography mass spectrometry (GC/MS) analysis. The influences of the main factors on the type and thickness of the homemade fi...

hcl- etched steel fiber for determination of phthalates in water samples by solid-phase microextraction